Assist. Prof. Dr. of Analytical Chemistry
Near East University, Department of Analytical Chemistry, Faculty of Pharmacy
Biography
Usama ALSHANA was born in 1977 in Khanyounis, Gaza Strip, Palestine. He graduated from Haroun Ar-Rasheed High School in 1995. He received his BSc. degree from Middle East Technical University, Department of Chemistry in 2001 and his MSc. degree in analytical chemistry from the same faculty in 2004. In 2013, he was awarded a Ph.D. degree from the Department of Analytical Chemistry, Faculty of Pharmacy at Gazi University. His Ph.D. thesis, supervised by Prof. Dr. Nusret ERTAŞ and Prof. Dr. O. Yavuz ATAMAN, was entitled ‘‘Speciation studies by capillary electrophoresis (CE) and high-performance liquid chromatography-hydride generation-atomic fluorescence spectrometry (HPLC-HG-AFS)’’. Dr. Usama ALSHANA joined the Faculty of Pharmacy at Near East University in September 2015 as Assist. Prof. Dr. of Analytical Chemistry and is currently the head of the Department of Analytical Chemistry. He is teaching theoretical and experimental analytical chemistry as well as conducting research with graduate students. His research interests include chromatographic and electrodriven separations, elemental speciation analysis, microextractions and green analytical chemistry.
Work Experience
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Todate 2015
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2015 2014
Assist. Prof. Dr. of Analytical Chemistry
Faculty of Engineering and Architecture, Avrasya University, Trabzon, Turkey., Department of Food Engineering,
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2015 2014
Deputy Director
Avrasya University, Trabzon, Turkey, Institute of Science and Technology
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2014 2004
Coordinator and Teacher of A-Level Chemistry
Affiliated with University of Cambridge, UK, Pakistan Embassy International Study Group, Ankara, Turkey
Education & Training
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Ph.D. 2013
Department of Analytical Chemistry, Faculty of Pharmacy
Gazi University
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Master2004
Department of Chemistry
Middle East Technical University
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Bachelor2001
Department of Chemistry
Middle East Technical University
Honors, Awards and Grants
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2001Republic of Turkey Prime Ministry, Bachelor Fellowship for Foreign Students, 1996–2001.
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2012The Scientific and Technological Research Council of Turkey (TÜBİTAK), Scientific Publications Incentive Award “Bilimsel Yayın Teşvik Ödülü”, 2012 (1).
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2007The Scientific and Technological Research Council of Turkey (TÜBİTAK), Ph.D. Fellowship for Foreign Country Citizens, 2007–2012.
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2013The Scientific and Technological Research Council of Turkey (TÜBİTAK), Scientific Publications Incentive Award “Bilimsel Yayın Teşvik Ödülü”, 2013 (2).
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2015The Scientific and Technological Research Council of Turkey (TÜBİTAK), Scientific Publications Incentive Award “Bilimsel Yayın Teşvik Ödülü”, 2015 (1).
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2009Republic of Turkey Ministry of Higher Education Ph.D. Fellowship for Foreign Students, 2009–2013.
Research Summary
Chromatographic and electrodriven separation sciences,
Elemental speciation analysis,
Microextractions,
Green analytical chemistry.
Interests
Research Projects
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ASSESSING THE HUMAN HEALTH RISKS FROM EXPOSURE OF ARSENIC IN DRINKING WATER THROUGH MOLECULAR EPIDEMIOLOGICAL APPROACHES. TÜBİTAK Proje No: 109S419, Proje Yürütücüsü: Prof.Dr. Sema BURGAZ This research has been carried out in three areas having different As levels in drinking water (>50?g/l; Dadağı, Küçükayhan, Emmiler and Gülpınar villages;10-50 ?g/l; Kızılkaya and Yassıca vilages; <10?g/l; as a control area; Eskiyaylacık, Civelek, Alkan and Altıpınar villages). 185 subjects from control area and 420 subjects from areas with As levels in water between 10 and >50 ?g/l have been involved in this study. Time-weighted average-As (TWA-As;µg/l ) levels in water have ranged from 62.10 and 134.30 for >50 µg/l As levels in water area, those from 18.33 and 36.39 for 10-50µg/l As levels in water area, those from 0.40 and 0.85 for control area. Urinary total As and total As species (AsIII, AsV, MMAV ve DMAV) levels of subjects living at As polluted water areas are significantly higher (p<0.001) than those of control subjects and also dose-related with As levels in water. As levels in hair samples indicate that chronic exposure to As is evident and drinking water is suggested to be principal factor for As exposure. As-induced genotoxicity parameters have been observed in peripheral lymphocytes and/or buccal cells from subjects living at areas with 10-50µg/l As and >50µg/l As in water. Our results indicate that As metabolism (DMA/MMA) is slightly influenced by AS3MT polymorphism. However, none of the other polymorphisms (GSTM1, GSTT1, GSTP1 ve GSTO1-1) affected As metabolism significantly. We do not observe elevated levels of skin lesions in subjects living in highly exposed As area and no effect of most of genetic polymorphisms on the frequency of skin lesions are found. In As exposed individuals only GSTT1 null genotype resulted increased buccal-MN frequency among all genotoxicity parameters. Based on lymphocyte-MN frequencies as a cancer predictivity marker revealed an increased genotoxicity risk in this region due to the As exposure. Therefore, it is crucial to give importance to cancer registry activities in the region.
Publications
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Separation and quantitation of some platinum group metals by high performance liquid chromatography
Conference Paper The 4th Aegean Analytical Chemistry Days (AACD) (Aydın, Turkey), Volume -, Issue -, 2004, Pages -
Abstract
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Özet
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Preconcentration of some precious metals using N,N-diethyl-N’-benzoylthiourea impregnated resin
Conference Paper The 4th Aegean Analytical Chemistry Days (AACD) (Aydın, Turkey), Volume -, Issue -, 2004, Pages -
Abstract
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Özet
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Separation and enrichment of platinum and palladium in soil, adapted to their determination by RP-HPLC
Conference Paper The 1st International Conference on Air Pollution and Combustion (Ankara, Turkey), Volume -, Issue -, 2005, Pages -
Abstract
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Özet
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Optimization of a HPLC method for separation of some platinum group metals
Conference Paper The 3rd Black Sea Basin Conference on Analytical Chemistry, Process Related Environmental Analytical Chemistry (Constanta, Romania), Volume -, Issue -, 2005, Pages -
Abstract
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Özet
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Separation and quantitation of Pt(II) and Pd(II) chelates with N,N-diethyl-N’-benzoylthiourea by reversed-phase high performance liquid chromatography
Conference Paper The 35th International Symposium on High Performance Liquid Phase Separations and Related Techniques ‘HPLC 2010’ (Boston, MA, USA), Volume -, Issue -, 2010, Pages -
Abstract
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Özet
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Separation, on-line preconcentration and speciation of arsenic and antimony by micellar electrokinetic chromatography
Conference Paper 5. Ulusal Analitik Kimya Kongresi (Erzurum, Turkey), Volume -, Issue -, 2010, Pages -
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Özet
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Speciation of arsenic and antimony by capillary electrophoresis
Conference Paper The 7th Aegean Analytical Chemistry Days (AACD) (Lesvos, Greece), Volume -, Issue -, 2010, Pages -
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Özet
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Solidification of organic drop microextraction combined with capillary electrophoresis for preconcentration and determination of bisphenol A in water samples
Conference Paper IMA 2011-Instrumental Methods of Analysis-Modern Trends and Applications (Chania, Crete, Greece), Volume -, Issue -, 2011, Pages -
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Özet
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Separation and determination of ephedrine, norephedrine and guaifenesin in pharmaceutical syrup and biological samples using micellar electrokinetic chromatography
Conference Paper IMA 2011-Instrumental Methods of Analysis-Modern Trends and Applications (Chania, Crete, Greece), Volume -, Issue -, 2011, Pages -
Abstract
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Özet
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Solidification of organic drop microextraction followed by online back-extraction in capillary electrophoresis
Conference Paper IMA 2011-Instrumental Methods of Analysis-Modern Trends and Applications (Chania, Crete, Greece), Volume -, Issue -, 2011, Pages -
Abstract
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Özet
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AS3MT gene polymorphism in residents exposed to inorganic arsenic via drinking water
Conference Paper EUROTOX 2012 (Stockholm, Sweden), Volume -, Issue -, 2012, Pages -
Abstract
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Özet
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Dispersive liquid-liquid microextraction based on solidification of floating organic drop combined with counter-electroosmotic flow normal stacking mode in capillary electrophoresis for the determination of bisphenol A in water and urine samples
Conference Paper VI. Ulusal Analitik Kimya Kongresi (Hatay, Turkey), Volume -, Issue -, 2012, Pages -
Abstract
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Özet
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Dispersive liquid-liquid microextraction combined with field-amplified sample stacking-capillary electrophoresis for the determination of non-steroidal anti-in?ammatory drugs in milk and dairy
Conference Paper VI. Ulusal Analitik Kimya Kongresi (Hatay, Turkey), Volume -, Issue -, 2012, Pages -
Abstract
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Özet
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A novel combination of dispersive liquid-liquid microextraction based on solidification of floating organic drop with field-amplified sample injection capillary electrophoresis for preconcentration and determination of beta(2)-agonists in bovine urine
Conference Paper VI. Ulusal Analitik Kimya Kongresi (Hatay, Turkey), Volume -, Issue -, 2012, Pages -
Abstract
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Özet
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Dispersive liquid-liquid microextraction combined with field-amplified sample stacking in capillary electrophoresis for the determination of non-steroidal anti-inflammatory drugs in milk and dairy products
Conference Paper The 8th Aegean Analytical Chemistry Days (AACD) (Izmir, Turkey), Volume -, Issue -, 2012, Pages -
Abstract
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Özet
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Speciation of urinary arsenic in Nevşehir area, Turkey, by high performance liquid chromatography coupled to hydride-generation atomic fluorescence spectrometry
Conference Paper The 8th Aegean Analytical Chemistry Days (AACD) (İzmir, Turkey), Volume -, Issue -, 2012, Pages -
Abstract
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Özet
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Determination of four beta(2)-agonists in bovine urine using dispersive liquid-liquid microextraction and gas chromatography-mass spectrometry
Conference Paper The 8th Aegean Analytical Chemistry Days (AACD) (İzmir, Turkey), Volume -, Issue -, 2012, Pages -
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Özet
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Kutu süt numunesinde alkilfenol bileşiklerinin dispersif sıvı-sıvı mikroekstraksiyon sonrası kapiler elektroforez ile tayini “Dispersive liquid-liquid microextraction of alkyphenols in bottled milk prior to field-amplified sample stacking in capillary electrophoresis”
Conference Paper XIII. Ulusal Spektroskopi Kongresi (Burdur, Turkey), Volume -, Issue -, 2013, Pages -
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Özet
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Nevşehir Bölgesinde Yaşayan İnsanların Saç Örneklerinde Toplam Arsenik Tayini “Total arsenic determination in hair samples from residents of Nevşehir Province, Turkey”
Conference Paper XIII. Ulusal Spektroskopi Kongresi (Burdur, Turkey), Volume -, Issue -, 2013, Pages -
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Özet
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Hair arsenic concentrations of residents living in Nevşehir province, Turkey
Conference Paper EUROTOX 2013 (Interlaken, Switzerland), Volume -, Issue -, 2013, Pages -
Abstract
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Özet
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Total arsenic determination in hair and urine samples from residents of Nevşehir Province, Turkey. Speciation studies in urine samples
Conference Paper IMA 2013-Instrumental Methods of Analysis-Modern Trends and Applications (Thessaloniki, Greece), Volume -, Issue -, 2013, Pages -
Abstract
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Özet
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Arsenic levels of residents of Nevşehir province, Turkey
Conference Paper The 5th International Congress on Arsenic in the Environment (As2014) (Buenos Aires, Argentina), Volume -, Issue -, 2014, Pages -
Abstract
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Özet
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Arsenic (+3) methyltransferase, and glutathione S-transferase omega genetic variants associated with arsenic susceptibility: Influences on As metabolism and skin lesions
Conference Paper SOT Annual Meeting (San Diego, USA), Volume -, Issue -, 2015, Pages -
Abstract
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Özet
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Optimization of a capillary electrophoresis method for the determination of antazoline and tetrahydrozoline in ophthalmic solutions
Conference Paper 11th International Symposium on Pharmaceutical Sciences (ISOPS-11) (Ankara, Turkey), Volume -, Issue -, 2015, Pages -
Abstract
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Özet
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Dispersive liquid-liquid microextraction as an efficient sample cleanup and preconcentration technique prior to capillary electrophoresis
Conference Paper International Multidisciplinary Symposium on Drug Research and Development (Eskişehir, Turkey), Volume -, Issue -, 2015, Pages -
Abstract
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Özet
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İçme sularında arsenik kirliliği olan bölgelerde yaşayan bireylerdeki sağlık risklerinin moleküler epidemiyolojik yöntemlerle araştırılması
Conference Paper Ulusal Su ve Sağlık Kongresi (Antalya, Turkey), Volume -, Issue -, 2015, Pages -
Abstract
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Özet
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Gene expression levels in individuals exposed to inorganic arsenic via drinking water
Conference Paper International Gazi Pharma symposium series (GPSS 2015) (Antalya, Turkey), Volume -, Issue -, 2015, Pages -
Abstract
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Özet
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Dispersive liquid-liquid microextraction prior to capillary electrophoresis for the determination of parabens in personal care products, human urine and saliva
Conference Paper International Gazi Pharma symposium series (GPSS 2015) (Antalya, Turkey), Volume -, Issue -, 2015, Pages -
Abstract
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Özet
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Dispersive liquid-liquid microextraction of caffeine from cola seeds and its quantitation using high-performance liquid chromatography
Conference Paper International Gazi Pharma symposium series (GPSS 2015) (Antalya, Turkey), Volume -, Issue -, 2015, Pages -
Abstract
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Özet
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The frequency of micronucleus and other nuclear anomalies in exfoliated buccal cells of individuals chronically exposed to low to moderate levels of arsenic via drinking water
Conference Paper International Gazi Pharma symposium series (GPSS 2015) (Antalya, Turkey), Volume -, Issue -, 2015, Pages -
Abstract
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Özet
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http://scholar.google.com/scholar?cluster=872634806232998657&hl=en&oi=scholarr
General Publication AS3MT gene polymorphism in residents exposed to inorganic arsenic via drinking water, 2016
Abstract
Özet
http://www.sciencedirect.com/science/article/pii/S0308814612018651
General Publication Dispersive liquid-liquid microextraction combined with field-amplified sample stacking in capillary electrophoresis for the determination of non-steroidal anti-inflammatory drugs in milk and dairy products, 2016
Abstract
Özet
http://www.sciencedirect.com/science/article/pii/S0308814615002642
General Publication Determination of parabens in human milk and other food samples by capillary electrophoresis after dispersive liquid–liquid microextraction with back-extraction, 2016
Abstract
Özet
http://www.crcnetbase.com/doi/abs/10.1201/b16767-213
General Publication One Century of the Discovery of Arsenicosis in Latin America (1914-2014) As2014, 2016
Abstract
Özet
https://www.infona.pl/resource/bwmeta1.element.elsevier-2923119a-768c-398e-99b8-8ae76540d9b4
General Publication Hair arsenic concentrations of residents living in Nevsehir province, Turkey, 2016
Abstract
Özet
http://onlinelibrary.wiley.com/doi/10.1002/elps.201200348/full
General Publication Dispersive liquid–liquid microextraction based on solidification of floating organic drop combined with field-amplified sample injection in capillary electrophoresis for the determination of beta(2)-agonists in bovine urine, 2016
Abstract
Özet
http://www.ingentaconnect.com/contentone/ben/cpa/2017/00000013/00000001/art00007
General Publication Quantification and Penetration Properties of p-Hydroxybenzoic Acid Derivatives, 2016
Abstract
Özet
http://onlinelibrary.wiley.com/doi/10.1002/jssc.201200308/full
General Publication Ultrasound-assisted emulsification microextraction for the determination of ephedrines in human urine by capillary electrophoresis with direct injection. Comparison with dispersive liquid–liquid microextraction, 2016
Abstract
Özet
http://www.tandfonline.com/doi/abs/10.1080/10826076.2011.570839
General Publication DETERMINATION OF PLATINUM AND PALLADIUM IN SOIL AS THEIR CHELATES WITH N, N-DIETHYL-N'-BENZOYLTHIOUREA BY RP-HPLC, 2016
Abstract
Özet
http://www.sciencedirect.com/science/article/pii/S0731708516300942
General Publication Determination of antazoline and tetrahydrozoline in ophthalmic solutions by capillary electrophoresis and stability-indicating HPLC methods, 2016
Abstract
Özet
http://www.tandfonline.com/doi/abs/10.1080/10826076.2012.725700
General Publication Dispersive liquid-liquid microextraction based on solidification of floating organic drop combined with counter-electroosmotic flow normal stacking mode in capillary electrophoresis for the determination of bisphenol A in water and urine samples, 2016
Abstract
Özet
Determination of platinum and palladium in soil as their chelates with N,N-Diethyl-N'-benzoylthiourea by RP-HPLC
Original Article . Journal of Liquid Chromatography & Related Technologies , Volume 34, Issue -, 2011, Pages 1326–1339
Abstract
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Özet
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AS3MT gene polymorphism in residents exposed to inorganic arsenic via drinking water
Original Article Toxicology Letters, Volume *, Issue -, 2012, Pages -
Abstract
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Özet
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Ultrasound-assisted emulsification microextraction for the determination of ephedrines in human urine by capillary electrophoresis with direct injection. Comparison with dispersive liquid–liquid microextraction
Original Article Journal of separation science, Volume *, Issue -, 2012, Pages -
Abstract
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Özet
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Dispersive liquid-liquid microextraction based on solidification of floating organic drop combined with counter-electroosmotic flow normal stacking mode in capillary electrophoresis for the determination of bisphenol A in water and urine samples
Original Article Journal of Liquid Chromatography & Related Technologies, Volume *, Issue -, 2013, Pages -
Abstract
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Özet
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Dispersive liquid–liquid microextraction based on solidification of floating organic drop combined with field-amplified sample injection in capillary electrophoresis for the determination of beta(2)-agonists in bovine urine
Original Article Electrophoresis, Volume *, Issue -, 2013, Pages -
Abstract
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Özet
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Hair arsenic concentrations of residents living in Nevsehir province, Turkey
Original Article Toxicology Letters, Volume *, Issue -, 2013, Pages -
Abstract
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Özet
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Dispersive liquid-liquid microextraction based on solidification of floating organic drop combined with counter-electroosmotic flow normal stacking mode in capillary electrophoresis for the determination of bisphenol A in water and urine samples
Original Article Journal of Liquid Chromatography & Related Technologies, Volume 36, Issue -, 2013, Pages 2855–2870
Abstract
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Özet
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Dispersive liquid-liquid microextraction combined with field-amplified sample stacking in capillary electrophoresis for the determination of non-steroidal anti-inflammatory drugs in milk and dairy products
Original Article Food Chemistry, Volume 138, Issue -, 2013, Pages 890–897
Abstract
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Özet
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Determination of parabens in human milk and other food samples by capillary electrophoresis after dispersive liquid–liquid microextraction with back-extraction
Original Article Food Chemistry, Volume 181, Issue -, 2015, Pages 1-8
Abstract
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Özet
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Teaching
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Currrent Teaching
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2018 BAHAR
ANALYTICAL CHEMISTRY LAB I*
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2018 BAHAR
ATOMİC SPECTROMETRY
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2018 BAHAR
INTRODUCTION TO ELECTROPHORETIC SEPARATIONS
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2018 BAHAR
ELECTROPHORESIS ANALYTICAL APPLICATIONS
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2018 BAHAR
CONTEMPORARY EXTRACTION TECHNIQUES
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2018 BAHAR
SEMINAR
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2018 BAHAR
THESIS
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Teaching History
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2016 BAHAR
CONTEMPORARY EXTRACTION TECHNIQUES
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2016 BAHAR
CAPILLARY ELECTROPHORESIS AND ANALYTICAL APPLICATIONS
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2018 GÜZ
ANALYTICAL CHEMISTRY I
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2018 GÜZ
ADVANCED ANALYTICAL CHEMISTRY
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2017 BAHAR
CONTEMPORARY EXTRACTION TECHNIQUES
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2015 GÜZ
CHROMATOGRAPHIC METHODS AND APPLICATIONS
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2017 BAHAR
NANOMATERIALS AND NANOTECHNOLOGY
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2018 GÜZ
PH.D. THESIS
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2017 GÜZ
MASTER THESIS
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2018 GÜZ
MASTER THESIS
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2018 GÜZ
SEMINAR
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2017 GÜZ
SEMINAR
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2016 GÜZ
ANALYTICAL CHEMISTRY II
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2016 BAHAR
SEMINAR
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2016 BAHAR
ANALYTICAL CHEMISTRY LAB I
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2017 YAZ
ANALYTICAL CHEMISTRY I*
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2017 BAHAR
ANALYTICAL CHEMISTRY I
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2017 BAHAR
ANALYTICAL CHEMISTRY I
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2017 GÜZ
ADVANCED ANALYTICAL CHEMISTRY
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2018 GÜZ
ADVANCED ANALYTICAL CHEMISTRY
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2017 GÜZ
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2018 GÜZ
SEPARATION TECHNIQUES
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2018 GÜZ
SEMINAR
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2015 BAHAR
ANALYTICAL CHEMISTRY LAB I
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2017 YAZ
ANALYTICAL CHEMISTRY II
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2016 BAHAR
INTRODUCTION TO ELECTROPHORETIC SEPARATIONS
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2017 GÜZ
ADVANCED ANALYTICAL CHEMISTRY (PHD)
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2018 GÜZ
ADVANCED ANALYTICAL CHEMISTRY (PHD)
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2017 BAHAR
MASTER THESIS
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ANALYTICAL CHEMISTRY LAB I*
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2017 GÜZ
INSTRUMENTAL METHODS
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2018 GÜZ
INSTRUMENTAL METHODS
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2017 GÜZ
PHARMACEUTICAL CHEMISTRY
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2015 GÜZ
SEPARATION TECHNIQUES
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2016 GÜZ
SEPARATION TECHNIQUES
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2017 GÜZ
GRADUATION PROJECT
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2018 GÜZ
GRADUATION PROJECT
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2017 BAHAR
ANALYTICAL CHEMISTRY LAB I
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2017 BAHAR
ANALYTICAL CHEMISTRY I*
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2017 BAHAR
INTRODUCTION TO ELECTROPHORETIC SEPARATIONS
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2016 GÜZ
ADVANCED ANALYTICAL CHEMISTRY
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2016 BAHAR
MASTER THESIS
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2015 BAHAR
ANALYTICAL CHEMISTRY I
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2015 GÜZ
ANALYTICAL CHEMISTRY II
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2016 GÜZ
GRADUATION PROJECT
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2017 GÜZ
CHROMATOGRAPHIC METHODS AND APPLICATIONS
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2018 GÜZ
CHROMATOGRAPHIC METHODS AND APPLICATIONS
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2017 GÜZ
ANALYTICAL CHEMISTRY LAB II
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2018 GÜZ
ANALYTICAL CHEMISTRY LAB II
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2016 BAHAR
ANALYTICAL CHEMISTRY I
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2016 BAHAR
NANOMATERIALS AND NANOTECHNOLOGY
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2016 GÜZ
CHROMATOGRAPHIC METHODS AND APPLICATIONS
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2016 GÜZ
ANALYTICAL CHEMISTRY LAB II
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2015 BAHAR
ANALYTICAL CHEMISTRY I*
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2017 BAHAR
ATOMIC SPECTROMETRY
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2015 BAHAR
INTRODUCTION TO ELECTROPHORETIC SEPARATIONS
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2017 GÜZ
ANALYTICAL CHEMISTRY II
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2018 GÜZ
ANALYTICAL CHEMISTRY II
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2016 BAHAR
ANALYTICAL CHEMISTRY LAB I*
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2015 GÜZ
SEPARATION TECHNIQUES
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2018 GÜZ
BASIC CONCEPTS IN ORGANIC CHEMISTRY
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2017 BAHAR
SCIENTIFIC RECORDING AND WRITING TECHNIQUES
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2016 GÜZ
ADVANCED ANALYTICAL CHEMISTRY (PHD)
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2015 GÜZ
CHROMATOGRAPHIC METHODS AND APPLICATIONS
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2015 GÜZ
ANALYTICAL CHEMISTRY LAB II
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2017 BAHAR
ANALYTICAL CHEMISTRY LAB I*
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2016 GÜZ
SEPARATION TECHNIQUES
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2016 GÜZ
CHROMATOGRAPHIC METHODS AND APPLICATIONS
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2016 BAHAR
ANALYTICAL CHEMISTRY I*
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2017 BAHAR
CAPILLARY ELECTROPHORESIS AND ANALYTICAL APPLICATIONS
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2016 GÜZ
CHROMOTOGRAPHIC METHODS AND APPLICATIONS
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